C₁₇H₂₀F₂N₄O

Base Information

Chemical Name:C₁₇H₂₀F₂N₄O
CAS No.:1292322-18-9
Molecular Formula:C₁₇H₂₀F₂N₄O
Molecular Weight:334.369
Hs Code.:

C<sub>17</sub>H<sub>20</sub>F<sub>2</sub>N<sub>4</sub>O

Synonyms:

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Chemical Property of C₁₇H₂₀F₂N₄O

Chemical Property:

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Technology Process of C₁₇H₂₀F₂N₄O

There total 13 articles about C₁₇H₂₀F₂N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₈F₂N₄O₃

: 1292322-18-9
C₁₇H₂₀F₂N₄O

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: C₁₄H₂₀Cl₃NO₅

: 1292322-18-9
C₁₇H₂₀F₂N₄O

Guidance literature:: Multi-step reaction with 10 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: hydrogenchloride / methanol / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

6: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

7: chloro-trimethyl-silane / dichloromethane / 20 °C

8: palladium 10% on activated carbon; hydrogen / ethanol

9: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; CyJohnPhos / toluene / 70 - 100 °C

10: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; CyJohnPhos; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 6: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 1292321-47-1
C₂₉H₃₄F₂N₂O₅

: 1292322-18-9
C₁₇H₂₀F₂N₄O

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / methanol / 20 °C

2: triethylamine / dichloromethane / 20 °C

3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

4: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

5: chloro-trimethyl-silane / dichloromethane / 20 °C

6: palladium 10% on activated carbon; hydrogen / ethanol

7: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; CyJohnPhos / toluene / 70 - 100 °C

8: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; CyJohnPhos; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060