3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione

Base Information

Chemical Name:3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione
CAS No.:1039453-20-7
Molecular Formula:C₂₃H₂₀N₄O₃
Molecular Weight:400.437
Hs Code.:

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Chemical Property of 3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione

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Technology Process of 3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione

There total 11 articles about 3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1039454-60-8
C₁₂H₁₄O₃S

: 1039453-19-4
6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione

: 1039453-20-7
3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione

Guidance literature:: With N,N-dimethyl acetamide; 1,8-diazabicyclo[5.4.0]undec-7-ene;

Reference yield:

: 1039453-63-8
C₁₂H₁₀N₂O₅

: 1039453-20-7
3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione

Guidance literature:: Multi-step reaction with 6 steps

1: potassium peroxymonosulfate / N,N-dimethyl-formamide / 18 h / 20 °C

2: thionyl chloride; N,N-dimethyl-formamide / chloroform / 0.5 - 18 h / 20 °C / Heating / reflux

3: ammonia / tetrahydrofuran; chloroform / 0.17 h

4: hydrogen / palladium 10% on activated carbon / chloroform; N,N-dimethyl-formamide / 24 h / 20 °C

5: isopentyl nitrite / N,N-dimethyl-formamide

6: N,N-dimethyl acetamide; 1,8-diazabicyclo[5.4.0]undec-7-ene

With potassium peroxymonosulfate; thionyl chloride; N,N-dimethyl acetamide; ammonia; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N-dimethyl-formamide; isopentyl nitrite; palladium 10% on activated carbon; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;

Reference yield:

: 1039453-60-5
6-methyl-3,3a-dihydro-1H-benzo[e]pyrrolo[2,1-b][1,3]oxazin-9(2H)-one

: 1039453-20-7
3-(1-phenylpent-3-yn-2-yl)-6a,7,8,9-tetrahydro-3H-pyrrolo[2',1':2,3][1,3]oxazino[6,5-g][1,2,3]benzotriazine-4,11-dione

Guidance literature:: Multi-step reaction with 8 steps

1.1: nitric acid; acetic anhydride; acetic acid / chloroform; water / 0.5 h / 0 °C

2.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 24 h / 125 °C

2.2: 0.25 h / 20 °C

3.1: potassium peroxymonosulfate / N,N-dimethyl-formamide / 18 h / 20 °C

4.1: thionyl chloride; N,N-dimethyl-formamide / chloroform / 0.5 - 18 h / 20 °C / Heating / reflux

5.1: ammonia / tetrahydrofuran; chloroform / 0.17 h

6.1: hydrogen / palladium 10% on activated carbon / chloroform; N,N-dimethyl-formamide / 24 h / 20 °C

7.1: isopentyl nitrite / N,N-dimethyl-formamide

8.1: N,N-dimethyl acetamide; 1,8-diazabicyclo[5.4.0]undec-7-ene

With potassium peroxymonosulfate; thionyl chloride; N,N-dimethyl acetamide; ammonia; hydrogen; nitric acid; acetic anhydride; acetic acid; N,N-dimethyl-formamide dimethyl acetal; 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N-dimethyl-formamide; isopentyl nitrite; palladium 10% on activated carbon; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;