[Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4)

Base Information

Chemical Name:[Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4)
CAS No.:675881-45-5
Molecular Formula:BF₄*C₂₈H₂₃O₂Ru₂
Molecular Weight:680.434
Hs Code.:

Synonyms:

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Chemical Property of [Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4)

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Technology Process of [Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4)

There total 1 articles about [Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: tetrafluoroboric acid

: 676255-60-0,675881-41-1
Ru2(CO)(μ-CO)(μ-η1,η3-C(C(phenyl)2OH)CHCH2)(η-C5H5)2

: 675881-45-5
[Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4)

Guidance literature:: In tetrahydrofuran; N2; addn. of tetrafluoroboric acid to THF soln. of the complex; pptn. by addn. of diethyl ether, washing the ppt. with diethyl ether, drying under reduced pressure; elem. anal.;
DOI:10.1016/S0020-1693(03)00391-8

Reference yield: 63.0%

: 675881-45-5
[Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4)

: 675881-39-7
[Ru2(CO)(μ-CO)(μ-η2,η2-(C(phenyl)2CCCH2)(η-C5H5)2]

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N2; addn. of the organic compd. to dichloromethane soln. of Ru complex, stirring for 5 min; solvent removal, chromy. (alumina, dichloromethane/hexane 1:9);
DOI:10.1016/S0020-1693(03)00391-8

Reference yield: 22.0%

: 675881-45-5
[Ru2(CO)(μ-CO)(μ-η2,η3-(C(phenyl)2CCHCH2)(η-C5H5)2](BF4)

: 675881-39-7
[Ru2(CO)(μ-CO)(μ-η2,η2-(C(phenyl)2CCCH2)(η-C5H5)2]

: 676255-77-9,675881-38-6
Ru2(CO)(μ-CO)(μ-η1,η3-(phenyl)2(methyl)CCHCH2)(η-C5H5)2

Guidance literature:: In tetrahydrofuran; diethyl ether; N2; addn. of excess methyl lithium to a THF suspn. of Ru complex, stirring for 0.5 h; solvent removal, chromy. (alumina, dichloromethane hexane 3:7 followed by 2:3);
DOI:10.1016/S0020-1693(03)00391-8