trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum

Base Information

Chemical Name:trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum
CAS No.:69058-37-3
Molecular Formula:C₁₆H₂₇Cl₃MoO₂P
Molecular Weight:484.662
Hs Code.:

Synonyms:

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Chemical Property of trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum

Chemical Property:

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Technology Process of trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum

There total 1 articles about trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 31355-55-2,39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

: 672-66-2
Dimethyl(phenyl)phosphine

: 69058-37-3,136982-74-6
trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum

Guidance literature:: In tetrahydrofuran; N2-atmosphere; stirring of Mo-complex with excess of phosphine (room temp.); pptn. on Et2O addn., filtration, washing (light petroleum), drying (vac.); elem. anal.;
DOI:10.1039/DT9780001139

Reference yield:

: 69058-37-3,136982-74-6
trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum

: 2999-74-8
dimethylmagnesium

: 69058-29-3
dimethyl(η6-benzene)bis(dimethylphenylphosphine)molybdenum(II)

Guidance literature:: With benzene; In tetrahydrofuran; benzene; N2-atmosphere; addn. of Mo-complex to mixt. of benzene/THF (2:1) contg. excess Me2Mg, stirring (room temp., 20-30 min); solvent removal (reduced pressure), extn. into light petroleum, filtration or centrifugation, solvent removal (reduced pressure), crystn. on cooling to -25°C; elem. anal.;
DOI:10.1039/DT9780001139

Reference yield:

: 69058-37-3,136982-74-6
trichlorobis(tetrahydrofuran)(dimethylphenylphosphine)molybdenum

: 95-47-6
o-xylene

: 2999-74-8
dimethylmagnesium

: 69058-31-7
dimethyl(η6-o-xylene)bis(dimethylphenylphosphine)molybdenum(II)

Guidance literature:: In tetrahydrofuran; N2-atmosphere; addn. of Mo-complex to mixt. of o-xylene/THF (2:1) contg.excess Me2Mg, stirring (room temp., 20-30 min); solvent removal (reduced pressure), extn. into light petroleum, filtration or centrifugation, solvent removal (reduced pressure), crystn. on cooling to -78°C; elem. anal.;
DOI:10.1039/DT9780001139