2-(5-arsenoso-2-nitro-phenoxy)-ethanol

Base Information

• Chemical Name: 2-(5-arsenoso-2-nitro-phenoxy)-ethanol
• CAS No.: 854228-49-2
• Molecular Formula: C₈H₈AsNO₅
• Molecular Weight: 273.077
• Mol file: 854228-49-2.mol

Synonyms:

Chemical Property of 2-(5-arsenoso-2-nitro-phenoxy)-ethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(5-arsenoso-2-nitro-phenoxy)-ethanol

There total 5 articles about 2-(5-arsenoso-2-nitro-phenoxy)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[3-(2-hydroxy-ethoxy)-4-nitro-phenyl]-arsonic acid (857578-87-1) → 2-(5-arsenoso-2-nitro-phenoxy)-ethanol (854228-49-2)

Guidance literature:

With hydrogenchloride; sulfur dioxide; hydrogen iodide; und Behandeln des Reaktionsprodukts mit wss.Natronlauge;

DOI:10.1021/ja01288a045

Reference yield:

2-(3-nitrophenoxy)ethanol (16365-26-7) → 2-(5-arsenoso-2-nitro-phenoxy)-ethanol (854228-49-2)

Guidance literature:

Multi-step reaction with 4 steps

1: Hydrogenation

2: water / Diazotization_.anschliessend mit alkal. wss. Natriumarsenit-Loesung unter Zusatz von Kupfer(II)-sulfat

3: nitric acid / anschliessend Erhitzen des Reaktionsgemisches mit wss. Salzsaeure

4: hydrogen iodide; aqueous hydrochloric acid; sulfur dioxide / und Behandeln des Reaktionsprodukts mit wss.Natronlauge

With hydrogenchloride; sulfur dioxide; water; hydrogen iodide; nitric acid;

DOI:10.1021/ja01288a045

Reference yield:

meta-nitrophenol (554-84-7) → 2-(5-arsenoso-2-nitro-phenoxy)-ethanol (854228-49-2)

Guidance literature:

Multi-step reaction with 5 steps

1: aqueous NaOH / auf Siedetemperatur

2: Hydrogenation

3: water / Diazotization_.anschliessend mit alkal. wss. Natriumarsenit-Loesung unter Zusatz von Kupfer(II)-sulfat

4: nitric acid / anschliessend Erhitzen des Reaktionsgemisches mit wss. Salzsaeure

5: hydrogen iodide; aqueous hydrochloric acid; sulfur dioxide / und Behandeln des Reaktionsprodukts mit wss.Natronlauge

With hydrogenchloride; sodium hydroxide; sulfur dioxide; water; hydrogen iodide; nitric acid;

DOI:10.1021/ja01288a045

upstream raw materials:

[3-(2-hydroxy-ethoxy)-4-nitro-phenyl]-arsonic acid

2-(3-nitrophenoxy)ethanol

meta-nitrophenol

3-(2-hydroxyethoxy)aniline