C₃₄H₅₃NO₁₂Si

Base Information

Chemical Name:C₃₄H₅₃NO₁₂Si
CAS No.:1379526-69-8
Molecular Formula:C₃₄H₅₃NO₁₂Si
Molecular Weight:695.88
Hs Code.:

C<sub>34</sub>H<sub>53</sub>NO<sub>12</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₅₃NO₁₂Si

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Technology Process of C₃₄H₅₃NO₁₂Si

There total 7 articles about C₃₄H₅₃NO₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₄₉NO₁₀Si

: 108-24-7
acetic anhydride

: 1379526-69-8
C₃₄H₅₃NO₁₂Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2cc32736h

Reference yield:

: C₃₃H₅₃NO₈Si

: 1379526-69-8
C₃₄H₅₃NO₁₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 18 h / 20 °C / Inert atmosphere; Molecular sieve

2: Oxone; 1,1,1-trifluoro-2-propanone; edetate disodium; sodium hydrogencarbonate / water; acetonitrile / 0.5 h / 0 °C / Inert atmosphere

3: indium(III) chloride / acetonitrile / 3 h / 20 °C / Inert atmosphere

4: dmap; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With dmap; indium(III) chloride; Oxone; 1,1,1-trifluoro-2-propanone; edetate disodium; sodium hydrogencarbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; acetonitrile; benzene;
DOI:10.1039/c2cc32736h

Reference yield:

: 1379526-65-4
C₃₃H₅₃NO₉Si

: 1379526-69-8
C₃₄H₅₃NO₁₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: Oxone; 1,1,1-trifluoro-2-propanone; edetate disodium; sodium hydrogencarbonate / water; acetonitrile / 0.5 h / 0 °C / Inert atmosphere

2: indium(III) chloride / acetonitrile / 3 h / 20 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With dmap; indium(III) chloride; Oxone; 1,1,1-trifluoro-2-propanone; edetate disodium; sodium hydrogencarbonate; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1039/c2cc32736h