8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one

Base Information

Chemical Name:8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one
CAS No.:51598-75-5
Molecular Formula:C₁₉H₁₄N₂O
Molecular Weight:286.333
Hs Code.:

8,13-dihydrobenzo<g>indolo<2,3-a>quinolizin-5(7H)-one

Synonyms:

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Chemical Property of 8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one

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Technology Process of 8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one

There total 4 articles about 8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98722-14-6
2-(2-(1H-indol-3-yl)ethyl)isoquinolin-1(2H)-one

: 51598-75-5
8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one

: 38752-99-7,39662-68-5
15,16,17,18,19,20-hexahydroyohimban-21-one

Guidance literature:: With boron trifluoride diethyl etherate; In acetonitrile; at 85 ℃; for 48h; Overall yield = 85 percent; Overall yield = 24 mg; Schlenk technique; Sealed tube;
DOI:10.1039/c9gc03629f

Reference yield:

: 119-65-3
isoquinoline

: 51598-75-5
8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one

: 38752-99-7,39662-68-5
15,16,17,18,19,20-hexahydroyohimban-21-one

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / Reflux

2: caesium carbonate; urea hydrogen peroxide adduct / dimethyl sulfoxide; N,N-dimethyl-formamide / 36 h / Cooling with ice; Green chemistry

3: boron trifluoride diethyl etherate / acetonitrile / 48 h / 85 °C / Schlenk technique; Sealed tube

With boron trifluoride diethyl etherate; urea hydrogen peroxide adduct; caesium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c9gc03629f

Reference yield:

: 111563-17-8
2-(2-(1H-indol-3-yl)ethyl)isoquinolin-2-ium iodide

: 51598-75-5
8,13-dihydrobenzoindolo<2,3-a>quinolizin-5(7H)-one

: 38752-99-7,39662-68-5
15,16,17,18,19,20-hexahydroyohimban-21-one

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; urea hydrogen peroxide adduct / dimethyl sulfoxide; N,N-dimethyl-formamide / 36 h / Cooling with ice; Green chemistry

2: boron trifluoride diethyl etherate / acetonitrile / 48 h / 85 °C / Schlenk technique; Sealed tube

With boron trifluoride diethyl etherate; urea hydrogen peroxide adduct; caesium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c9gc03629f