[1-carbonyl-1-(η(5)-cyclopentadienyl)-3-methyl-2,2-diphenyl-1-trimethylphosphine-3-trimethylphosphoranylidene-1-tungsta-2-phosphacyclopropane] hexafluorophosphate

Base Information

• Chemical Name: [1-carbonyl-1-(η(5)-cyclopentadienyl)-3-methyl-2,2-diphenyl-1-trimethylphosphine-3-trimethylphosphoranylidene-1-tungsta-2-phosphacyclopropane] hexafluorophosphate
• CAS No.: 164987-09-1
• Molecular Formula: C₂₆H₃₆OP₃W*F₆P
• Molecular Weight: 786.307

Synonyms:

Chemical Property of [1-carbonyl-1-(η(5)-cyclopentadienyl)-3-methyl-2,2-diphenyl-1-trimethylphosphine-3-trimethylphosphoranylidene-1-tungsta-2-phosphacyclopropane] hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of [1-carbonyl-1-(η(5)-cyclopentadienyl)-3-methyl-2,2-diphenyl-1-trimethylphosphine-3-trimethylphosphoranylidene-1-tungsta-2-phosphacyclopropane] hexafluorophosphate

There total 1 articles about [1-carbonyl-1-(η(5)-cyclopentadienyl)-3-methyl-2,2-diphenyl-1-trimethylphosphine-3-trimethylphosphoranylidene-1-tungsta-2-phosphacyclopropane] hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

{carbonyl(η5-cyclopentadienyl)(η2-diphenylphosphino-methylcarben)trimethylphosphinetungsten} hexafluorophosphate + trimethylphosphane (594-09-2) → [1-carbonyl-1-(η(5)-cyclopentadienyl)-3-methyl-2,2-diphenyl-1-trimethylphosphine-3-trimethylphosphoranylidene-1-tungsta-2-phosphacyclopropane] hexafluorophosphate (164987-09-1)

Guidance literature:

In dichloromethane; N2-atmosphere; addn. of excess PMe3 to W-complex at -40°C, standing at room temp. for 10 h; pptn. from CH2Cl2/pentane, repeated recrystn. (CH2Cl2/pentane), drying (vac.); elem. anal.;

DOI:10.1016/0022-328X(94)05246-8

upstream raw materials:

trimethylphosphane

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