N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester

Base Information

Chemical Name:N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester
CAS No.:34897-64-8
Molecular Formula:C₃₂H₃₄N₂O₉
Molecular Weight:590.63
Hs Code.:

<i>N</i>-(<i>O</i>-benzyl-<i>N</i>-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester

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Chemical Property of N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester

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Technology Process of N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester

There total 8 articles about N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3705-42-8
Cbz-(L)-Glu-OBn

: 34897-64-8
N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester

Guidance literature:: With 1,4-dioxane; tributyl-amine; chloroformic acid ethyl ester; anschliessend Behandeln mit L-Glutaminsaeure-1-benzylester und K₂CO₃ in wss. Dioxan;
DOI:10.1021/ja01636a024

Reference yield:

: 98102-32-0
(S)-1-benzyl 5-tert-butyl 2-aminopentanedioate hydrochloride

: 34897-64-8
N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / CH₂Cl₂

2: CF₃CO₂H / Ambient temperature

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/P19720000605

Reference yield:

: 53363-74-9
N-Z-L-Glu-OBzl-γ-Dcha salt

: 34897-64-8
N-(O-benzyl-N-benzyloxycarbonyl-L-γ-glutamyl)-L-glutamic acid-1-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / CH₂Cl₂

2: CF₃CO₂H / Ambient temperature

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/P19720000605