3-hydroxy-α-damascone

Base Information

• Chemical Name: 3-hydroxy-α-damascone
• CAS No.: 132620-72-5
• Molecular Formula: C₁₃H₂₀O₂
• Molecular Weight: 208.301

Synonyms:

Chemical Property of 3-hydroxy-α-damascone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-hydroxy-α-damascone

There total 5 articles about 3-hydroxy-α-damascone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-damascone (24720-09-0) → 3-hydroxy-α-damascone (51769-15-4,132620-72-5,132620-73-6) + (E)-megastigma-4,8-diene-3,7-dione (43126-29-0,865083-88-1)

Guidance literature:

With dihydrogen peroxide; recombinant unspecific peroxygenase from Daldinia caldariorum; In aq. phosphate buffer; at 30 ℃; for 0.0833333h; pH=7; diastereoselective reaction; Enzymatic reaction;

DOI:10.1021/acs.jafc.0c01019

Reference yield:

α-damascone (24720-09-0) → 3-hydroxy-α-damascone (51769-15-4,132620-72-5,132620-73-6) + 4-oxo-4-(2,6,6-trimethylcyclohex-2-en-1-yl)but-2-enoic acid

Guidance literature:

With dihydrogen peroxide; unspecific peroxygenase (isoform II) from Agrocybe aegerita TM-A₁; In aq. phosphate buffer; at 30 ℃; for 0.5h; pH=7; diastereoselective reaction; Enzymatic reaction;

DOI:10.1021/acs.jafc.0c01019

Reference yield:

α-damascone (24720-09-0) → 2,6,6-trimethyl-2,3-epoxy-1-(but-2-enoyl)cyclohexan + 3-hydroxy-α-damascone (51769-15-4,132620-72-5,132620-73-6) + (E)-megastigma-4,8-diene-3,7-dione (43126-29-0,865083-88-1)

Guidance literature:

With unspecific peroxygenase from Chaetomium globosum DSM-62110; dihydrogen peroxide; In aq. phosphate buffer; at 30 ℃; for 0.5h; pH=7; diastereoselective reaction; Enzymatic reaction;

DOI:10.1021/acs.jafc.0c01019

upstream raw materials:

α-damascone

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