C₂₃H₂₀FN₅O

Base Information

Chemical Name:C₂₃H₂₀FN₅O
CAS No.:1357089-43-0
Molecular Formula:C₂₃H₂₀FN₅O
Molecular Weight:401.443
Hs Code.:

C<sub>23</sub>H<sub>20</sub>FN<sub>5</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₀FN₅O

Chemical Property:

Purity/Quality:

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Technology Process of C₂₃H₂₀FN₅O

There total 9 articles about C₂₃H₂₀FN₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312579-10-4
C₂₆H₂₈BrN₃O₆

: 1357089-43-0
C₂₃H₂₀FN₅O

Guidance literature:: Multi-step reaction with 6 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane / 1 h

2: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / 0 °C

3: potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex / 1,4-dioxane / 6 h / 100 °C

4: trichlorophosphate / 2 h / 100 °C

5: tetrahydrofuran / 2 h / Reflux

6: 1-(Trimethylsilyl)imidazole / dichloromethane / 1 h

With triethylsilane; potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex; 1-(Trimethylsilyl)imidazole; trifluoroacetic acid; lithium hexamethyldisilazane; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2011.11.113

Reference yield:

: 1357089-55-4
C₂₄H₂₂BrN₃O₄

: 1357089-43-0
C₂₃H₂₀FN₅O

Guidance literature:: Multi-step reaction with 4 steps

1: potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex / 1,4-dioxane / 6 h / 100 °C

2: trichlorophosphate / 2 h / 100 °C

3: tetrahydrofuran / 2 h / Reflux

4: 1-(Trimethylsilyl)imidazole / dichloromethane / 1 h

With potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex; 1-(Trimethylsilyl)imidazole; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2011.11.113

Reference yield:

: 1312579-11-5
C₂₆H₂₈BrN₃O₅

: 1357089-43-0
C₂₃H₂₀FN₅O

Guidance literature:: Multi-step reaction with 5 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / 0 °C

2: potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex / 1,4-dioxane / 6 h / 100 °C

3: trichlorophosphate / 2 h / 100 °C

4: tetrahydrofuran / 2 h / Reflux

5: 1-(Trimethylsilyl)imidazole / dichloromethane / 1 h

With potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex; 1-(Trimethylsilyl)imidazole; lithium hexamethyldisilazane; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2011.11.113