<1-Hydroxy-5-chlor-8-methoxy-9-oxo-3,3a,4,9-tetrahydro-2H-benz(f)-indenyliden-(2)>-glykolsaeurebenzylester

Base Information

Chemical Name:<1-Hydroxy-5-chlor-8-methoxy-9-oxo-3,3a,4,9-tetrahydro-2H-benz(f)-indenyliden-(2)>-glykolsaeurebenzylester
CAS No.:17797-79-4
Molecular Formula:C₂₃H₁₉ClO₆
Molecular Weight:426.853
Hs Code.:

Synonyms:

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Chemical Property of <1-Hydroxy-5-chlor-8-methoxy-9-oxo-3,3a,4,9-tetrahydro-2H-benz(f)-indenyliden-(2)>-glykolsaeurebenzylester

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Technology Process of <1-Hydroxy-5-chlor-8-methoxy-9-oxo-3,3a,4,9-tetrahydro-2H-benz(f)-indenyliden-(2)>-glykolsaeurebenzylester

There total 8 articles about <1-Hydroxy-5-chlor-8-methoxy-9-oxo-3,3a,4,9-tetrahydro-2H-benz(f)-indenyliden-(2)>-glykolsaeurebenzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5368-81-0
methyl 3-methoxybenzoate

: 17797-79-4
<1-Hydroxy-5-chlor-8-methoxy-9-oxo-3,3a,4,9-tetrahydro-2H-benz(f)-indenyliden-(2)>-glykolsaeurebenzylester

Guidance literature:: Multi-step reaction with 8 steps

1: NaH

2: NaH

3: aq. H₂SO₄, AcOH / Heating

4: H₂SO₄

5: (i) H₂, Pd-C, (ii) /BRN= 1098229/, H₂SO₄

6: (i) aq. NaOH, (ii) Cl₂, I₂, AcOH, (iii) HF

7: H₂SO₄

8: NaH

With sulfuric acid; sodium hydride; acetic acid;
DOI:10.1021/ja01004a041

Reference yield:

: 795-17-5
β-(3-Methoxybenzyl)-adipinsaeure-dimethylester

: 17797-79-4
<1-Hydroxy-5-chlor-8-methoxy-9-oxo-3,3a,4,9-tetrahydro-2H-benz(f)-indenyliden-(2)>-glykolsaeurebenzylester

Guidance literature:: Multi-step reaction with 3 steps

1: (i) aq. NaOH, (ii) Cl₂, I₂, AcOH, (iii) HF

2: H₂SO₄

3: NaH

With sulfuric acid; sodium hydride;
DOI:10.1021/ja01004a041