Technology Process of C31H47O3P
There total 14 articles about C31H47O3P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Br(1-)*C37H52O2P(1+);
With
sodium hexamethyldisilazane;
In
tetrahydrofuran;
at 20 ℃;
C31H60O;
In
tetrahydrofuran;
at -84 ℃;
diastereoselective reaction;
DOI:10.1016/j.tetlet.2011.11.021
- Guidance literature:
-
Br(1-)*C37H52O2P(1+);
With
sodium hexamethyldisilazane;
In
tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone;
at 20 ℃;
With
C31H60O;
In
tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone;
at -84 ℃;
DOI:10.1016/j.tetlet.2011.11.021
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid; water; hydrogen bromide / 110 °C
2.1: acetonitrile / 170 °C / Microwave irradiation
3.1: sodium hexamethyldisilazane / tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 20 °C
3.2: -84 °C
With
sulfuric acid; water; hydrogen bromide; sodium hexamethyldisilazane;
In
tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.021