Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester

Base Information

• Chemical Name: Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester
• CAS No.: 171081-33-7
• Molecular Formula: C₄₁H₃₈FN₆O₇P
• Molecular Weight: 776.761

Synonyms:

Chemical Property of Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester

Chemical Property:

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Technology Process of Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester

There total 1 articles about Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Hydroxypropionitrile (109-78-4) + C44H48FN6O6P → Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester (171081-33-7)

Guidance literature:

With 1H-tetrazole; In acetonitrile; for 0.166667h; Ambient temperature;

DOI:10.1246/cl.1995.727

Reference yield:

Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester (171081-33-7) → Phosphorofluoridic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester

Guidance literature:

With tert.-butylhydroperoxide;

DOI:10.1246/cl.1995.727

Reference yield:

Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl ester 2-cyano-ethyl ester (171081-33-7) → Thiophosphorofluoridic acid O-{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-tetrahydro-furan-2-ylmethyl} ester O'-(2-cyano-ethyl) ester

Guidance literature:

With sulfur;

DOI:10.1246/cl.1995.727

upstream raw materials:

3-Hydroxypropionitrile

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