C₃₉H₄₇N₅O₅

Base Information

Chemical Name:C₃₉H₄₇N₅O₅
CAS No.:1275033-98-1
Molecular Formula:C₃₉H₄₇N₅O₅
Molecular Weight:665.833
Hs Code.:

C<sub>39</sub>H<sub>47</sub>N<sub>5</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₄₇N₅O₅

Chemical Property:

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Technology Process of C₃₉H₄₇N₅O₅

There total 7 articles about C₃₉H₄₇N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1275033-97-0
C₃₉H₄₇N₅O₅

: 1275033-98-1
C₃₉H₄₇N₅O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / -20 °C

1.2: -20 - 20 °C

2.1: acetic acid / 2 h / 50 °C

3.1: potassium acetate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 80 °C / Inert atmosphere

4.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 85 °C / Inert atmosphere

5.1: potassium acetate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / dimethyl sulfoxide / 80 °C / Inert atmosphere

6.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 15 h / 97 °C / Inert atmosphere

With potassium acetate; chloroformic acid ethyl ester; sodium hydrogencarbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; dimethyl sulfoxide;

Reference yield:

: 1575-37-7
4-Bromo-benzene-1,2-diamine

: 1275033-97-0
C₃₉H₄₇N₅O₅

: 1275033-98-1
C₃₉H₄₇N₅O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / -20 °C

1.2: -20 - 20 °C

2.1: acetic acid / 2 h / 50 °C

3.1: potassium acetate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 80 °C / Inert atmosphere

4.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 85 °C / Inert atmosphere

5.1: potassium acetate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / dimethyl sulfoxide / 80 °C / Inert atmosphere

6.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 15 h / 97 °C / Inert atmosphere

With potassium acetate; chloroformic acid ethyl ester; sodium hydrogencarbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; dimethyl sulfoxide;

Reference yield:

: 1228553-72-7
(2S)-1-tert-butoxycarbonyl-2-(2-amino-4-bromophenylaminoacyl)pyrrolidine

: 1275033-97-0
C₃₉H₄₇N₅O₅

: 1275033-98-1
C₃₉H₄₇N₅O₅

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 2 h / 50 °C

2: potassium acetate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 80 °C / Inert atmosphere

3: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 85 °C / Inert atmosphere

4: potassium acetate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / dimethyl sulfoxide / 80 °C / Inert atmosphere

5: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 15 h / 97 °C / Inert atmosphere

With potassium acetate; sodium hydrogencarbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,4-dioxane; 1,2-dimethoxyethane; water; dimethyl sulfoxide;