Technology Process of C35H24F6N2O2S2
There total 12 articles about C35H24F6N2O2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1039/c1jm12707a
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: toluene-4-sulfonic acid / toluene / Reflux
2.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 °C / Inert atmosphere
2.3: Inert atmosphere; Reflux
3.1: hydrogenchloride; water / tetrahydrofuran; hexane / Inert atmosphere
4.1: bromine / chloroform; acetonitrile / 6 h / Reflux
5.1: toluene-4-sulfonic acid / toluene
6.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere
6.2: 4.5 h / -78 °C / Inert atmosphere
7.1: pyridinium p-toluenesulfonate / acetone / Reflux
8.1: potassium borohydride / ethanol; water / 20 °C
9.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C
With
hydrogenchloride; dmap; n-butyllithium; potassium borohydride; water; bromine; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; ethanol; hexane; chloroform; water; acetone; toluene; acetonitrile;
DOI:10.1039/c1jm12707a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere
1.2: 4.5 h / -78 °C / Inert atmosphere
2.1: pyridinium p-toluenesulfonate / acetone / Reflux
3.1: potassium borohydride / ethanol; water / 20 °C
4.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C
With
dmap; n-butyllithium; potassium borohydride; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; ethanol; hexane; water; acetone;
DOI:10.1039/c1jm12707a