(S)-(+)-4--α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol

Base Information

Chemical Name:(S)-(+)-4--α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol
CAS No.:125345-93-9
Molecular Formula:C₂₅H₂₆F₂N₆OS
Molecular Weight:496.584
Hs Code.:

(S)-(+)-4-<bis(4-fluorophenyl)methyl>-α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(+)-4--α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol

Chemical Property:

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Technology Process of (S)-(+)-4--α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol

There total 2 articles about (S)-(+)-4--α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27469-60-9
1-(4-fluorophenyl)methyl-piperazine

: 125345-93-9
(S)-(+)-4--α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 50percent NaH / tetrahydrofuran / 20 h / Ambient temperature

2: 1.) 50percent NaH / 1.) DMF, 5 deg C, 20 min, 2.) DMF, RT, 72 h

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0957-4166(00)82104-7

Reference yield:

: 125411-48-5
(S)-(-)-1--4-(oxiranylmethyl)piperazine

: 157930-09-1,157930-10-4,157930-11-5,157930-13-7,157930-14-8
6-Mercaptopurine

: 125345-93-9
(S)-(+)-4--α-<(1H-purin-6-ylthio)methyl>-1-piperazineethanol

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 5 deg C, 20 min, 2.) DMF, RT, 72 h;
DOI:10.1016/S0957-4166(00)82104-7