(2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate

Base Information

Chemical Name:(2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate
CAS No.:1384982-23-3
Molecular Formula:C₅₆H₅₅O₁₆P
Molecular Weight:1015.02
Hs Code.:

(2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate

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Chemical Property of (2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate

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Technology Process of (2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate

There total 6 articles about (2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₆H₅₈BO₁₅P

: 1384982-23-3
(2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate

: 1384982-24-4
(2R,3R,4S,5R,6S)-2-((((2R,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyl tribenzoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo400864s

Reference yield:

: C₃₀H₄₂BO₇P

: 1384982-23-3
(2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate

: 1384982-24-4
(2R,3R,4S,5R,6S)-2-((((2R,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyl tribenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / methanol / 3.75 h / 20 °C / Inert atmosphere

2.1: iodine; pyridine / 4 h / 20 °C / Inert atmosphere

3.1: thiophenol / tetrahydrofuran / 20 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

4.2: 20 °C / Molecular sieve; Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With pyridine; dmap; iodine; sodium methylate; thiophenol; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo400864s

Reference yield:

: (2S,3S,4S,5S,6R)-2-boranyl-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-methoxy-1,2-oxaphosphinan-3-ol

: 1384982-23-3
(2R,3R,5R,6S)-2-((((2S,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyltribenzoate

: 1384982-24-4
(2R,3R,4S,5R,6S)-2-((((2R,3S,4S,5S,6R)-3-acetoxy-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-oxido-1,2-oxaphosphinan-2-yl)oxy)methyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triyl tribenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: iodine; pyridine / 4 h / 20 °C / Inert atmosphere

2.1: thiophenol / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 20 °C / Molecular sieve; Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With pyridine; dmap; iodine; thiophenol; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo400864s