benzylmagnesium chloride-d7

Base Information

Chemical Name:benzylmagnesium chloride-d7
CAS No.:1244030-76-9
Molecular Formula:C₇H₇ClMg
Molecular Weight:157.835
Hs Code.:

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Chemical Property of benzylmagnesium chloride-d7

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Technology Process of benzylmagnesium chloride-d7

There total 1 articles about benzylmagnesium chloride-d7 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 59502-05-5
benzyl chloride-d7

: 1244030-76-9
benzylmagnesium chloride-d7

Guidance literature:: With magnesium; ethylene dibromide; In tetrahydrofuran; for 1h; Schlenk technique; Reflux;
DOI:10.1002/chem.202000840

Reference yield: 66.0%

: 1244030-76-9
benzylmagnesium chloride-d7

: W(N-2,6-dichlorophenyl)(OtBu)₂Cl₂

: W(N-2,6-dichlorophenyl)(CD₂C₆D₅)₂(O^tBu)₂

Guidance literature:: In tetrahydrofuran; diethyl ether; at -35 ℃; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1002/chem.202000840

Reference yield: 26.0%

: 1244030-76-9
benzylmagnesium chloride-d7

: [bis(1,2,4-tri-t-butylcyclopentadienyl)cerium](CF₃SO₃)*0.5C₆H₁₄

: 1002717-01-2
bis(1,2,4-tri-t-butylcyclopentadienyl)cerium chloride

: 1244030-77-0
(C₅H₂(C(CH₃)3)3)2CeC⁽²⁾H₂C₆⁽²⁾H₅

Guidance literature:: In dichloromethane; (Schlenk, inert atm.) Mg-compound in diethyl ether was added to a soln. of complex in diethyl ether, 5 min; the solvent was removed under reduced pressure, extd. with pentane, reduced in vol., cooled to -10°C;
DOI:10.1039/b918103b