C₂₀H₃₂OSi

Base Information

Chemical Name:C₂₀H₃₂OSi
CAS No.:1400915-69-6
Molecular Formula:C₂₀H₃₂OSi
Molecular Weight:316.559
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₃₂OSi

Chemical Property:

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Technology Process of C₂₀H₃₂OSi

There total 3 articles about C₂₀H₃₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1400914-99-9
C₂₀H₃₉BO₃Si

: 1400915-69-6
C₂₀H₃₂OSi

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In water; toluene; at 100 ℃; for 6h;
DOI:10.1021/ja3070717

Reference yield:

: 693-02-7
hex-1-yne

: 1400915-69-6
C₂₀H₃₂OSi

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; diethylamine / 12 h / 20 °C / Inert atmosphere; Cooling with ice

2: palladium(II) acetylacetonate; triethylphosphine; diisobutylaluminium hydride / toluene / 24 h / 20 °C / Inert atmosphere; Glovebox

3: pyridine / toluene / 12 h / 20 °C / Inert atmosphere; Glovebox

4: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / toluene; water / 6 h / 100 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; pyridine; palladium(II) acetylacetonate; potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; diisobutylaluminium hydride; diethylamine; triethylphosphine; In water; toluene;
DOI:10.1021/ja3070717

Reference yield:

: 56392-46-2,90644-60-3
(Z)-non-2-en-4-yne

: 1400915-69-6
C₂₀H₃₂OSi

Guidance literature:: Multi-step reaction with 3 steps

1: palladium(II) acetylacetonate; triethylphosphine; diisobutylaluminium hydride / toluene / 24 h / 20 °C / Inert atmosphere; Glovebox

2: pyridine / toluene / 12 h / 20 °C / Inert atmosphere; Glovebox

3: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / toluene; water / 6 h / 100 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; pyridine; palladium(II) acetylacetonate; potassium phosphate; palladium diacetate; diisobutylaluminium hydride; triethylphosphine; In water; toluene;
DOI:10.1021/ja3070717