Technology Process of C29H37F2NO5
There total 13 articles about C29H37F2NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: cis-nitrous acid; potassium iodide / ethanol
2: borane / tetrahydrofuran
3: sodium tris(acetoxy)borohydride / dichloromethane
With
borane; cis-nitrous acid; sodium tris(acetoxy)borohydride; potassium iodide;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.01.014
- Guidance literature:
-
Multi-step reaction with 6 steps
1: caesium carbonate / N,N-dimethyl-formamide / 100 °C
2: methanol / diethyl ether
3: palladium on activated charcoal; hydrogen / ethanol
4: cis-nitrous acid; potassium iodide / ethanol
5: borane / tetrahydrofuran
6: sodium tris(acetoxy)borohydride / dichloromethane
With
methanol; palladium on activated charcoal; borane; hydrogen; cis-nitrous acid; sodium tris(acetoxy)borohydride; caesium carbonate; potassium iodide;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.01.014
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane
2: lithium diisopropyl amide
3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water
4: diphenyl phosphoryl azide; triethylamine / toluene
5: palladium on activated charcoal; hydrogen / methanol
6: sodium tris(acetoxy)borohydride / dichloromethane
With
diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; sodium tris(acetoxy)borohydride; triethylamine; lithium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene;
2: Evan's asymmetric alkylation / 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.01.014