Technology Process of C24H30NO10S(1-)*Na(1+)
There total 5 articles about C24H30NO10S(1-)*Na(1+) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid / 5 h / 50 °C
2.1: di(n-butyl)tin oxide / toluene / 5 h
2.2: 36 h / 70 °C
3.1: pyridine / 1,2-dichloro-ethane / 2 h / -15 °C
4.1: tetrabutylammonium nitrite / N,N-dimethyl-formamide / 3 h / 20 °C
5.1: pyridine; sulfur trioxide pyridine complex / 1 h / 65 °C
With
pyridine; sulfur trioxide pyridine complex; di(n-butyl)tin oxide; acetic acid; tetrabutylammonium nitrite;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2012.03.033
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: di(n-butyl)tin oxide / toluene / 5 h
1.2: 36 h / 70 °C
2.1: pyridine / 1,2-dichloro-ethane / 2 h / -15 °C
3.1: tetrabutylammonium nitrite / N,N-dimethyl-formamide / 3 h / 20 °C
4.1: pyridine; sulfur trioxide pyridine complex / 1 h / 65 °C
With
pyridine; sulfur trioxide pyridine complex; di(n-butyl)tin oxide; tetrabutylammonium nitrite;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2012.03.033
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 1,2-dichloro-ethane / 2 h / -15 °C
2: tetrabutylammonium nitrite / N,N-dimethyl-formamide / 3 h / 20 °C
3: pyridine; sulfur trioxide pyridine complex / 1 h / 65 °C
With
pyridine; sulfur trioxide pyridine complex; tetrabutylammonium nitrite;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.03.033
