Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄)

Base Information

Chemical Name:Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄)
CAS No.:1377605-03-2
Molecular Formula:C₂₅H₄₀N₃O₂P₂Rh
Molecular Weight:579.465
Hs Code.:

Rh(2,6-(CH<sub>2</sub>-PiPr<sub>2</sub>)2C<sub>5</sub>H<sub>3</sub>N)(p-NO<sub>2</sub>-NHC<sub>6</sub>H<sub>4</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄)

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Technology Process of Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄)

There total 3 articles about Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1377604-96-0
[Rh(2,6-(CH₂-PiPr₂)2C₅H₂N)(C₂H₄)]

: 100-01-6,104810-17-5
4-nitro-aniline

: 1377605-03-2
Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄)

Guidance literature:: (under N2, Schlenk); Rh-complex placed in NMR tube, benzene-d6 or THF soln. of p-nitroaniline added, heated at 60°C for 1 h; solvent removed in vac.; elem. anal.;
DOI:10.1021/om300248r

Reference yield:

: 62-53-3
aniline

: 1377605-03-2
Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄)

Guidance literature:: Multi-step reaction with 2 steps

2: tetrahydrofuran

In tetrahydrofuran;
DOI:10.1021/om300248r

Reference yield:

: 1377605-02-1
Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(NHC₆H₅)

: 100-01-6,104810-17-5
4-nitro-aniline

: 1377605-03-2
Rh(2,6-(CH₂-PiPr₂)2C₅H₃N)(p-NO₂-NHC₆H₄)

Guidance literature:: In tetrahydrofuran; (under N2, Schlenk); p-nitroaniline added to THF suspn. of Rh-complex inNMR tube, heated at 60°C for 20 h; monitored by NMR;
DOI:10.1021/om300248r