C₄₇H₃₁N*ClH

Base Information

• Chemical Name: C₄₇H₃₁N*ClH
• CAS No.: 1619936-07-0
• Molecular Formula: C₄₇H₃₁N*ClH
• Molecular Weight: 646.231
• Mol file: 1619936-07-0.mol

Synonyms:

Chemical Property of C₄₇H₃₁N*ClH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₇H₃₁N*ClH

There total 3 articles about C₄₇H₃₁N*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(naphthalen-1-yl)isoquinoline (52134-87-9,66920-31-8) → C47H31N*ClH (1619936-07-0)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; silver hexafluoroantimonate / tert-Amyl alcohol / 12 h / 120 °C / Sealed tube; Inert atmosphere

2: acetyl chloride / diethyl ether / Inert atmosphere

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; acetyl chloride; In tert-Amyl alcohol; diethyl ether;

DOI:10.1039/c4cc02822h

Reference yield:

diphenyl acetylene (501-65-5) → C47H31N*ClH (1619936-07-0)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; silver hexafluoroantimonate / tert-Amyl alcohol / 12 h / 120 °C / Sealed tube; Inert atmosphere

2: acetyl chloride / diethyl ether / Inert atmosphere

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; acetyl chloride; In tert-Amyl alcohol; diethyl ether;

DOI:10.1039/c4cc02822h

Reference yield:

C47H31N (1619935-89-5) → C47H31N*ClH (1619936-07-0)

Guidance literature:

With acetyl chloride; In diethyl ether; Inert atmosphere;

DOI:10.1039/c4cc02822h

upstream raw materials:

1-(naphthalen-1-yl)isoquinoline

diphenyl acetylene

C₄₇H₃₁N