(9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate

Base Information

Chemical Name:(9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate
CAS No.:1365565-34-9
Molecular Formula:C₃₂H₃₈N₄O₇
Molecular Weight:590.676
Hs Code.:

Synonyms:

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Chemical Property of (9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate

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Technology Process of (9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate

There total 13 articles about (9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1365565-34-9
(9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 20 °C

2: benzene / 32 h / 80 °C / Inert atmosphere

3: hydrogenchloride; water / methanol

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; benzene;
DOI:10.1021/jo2025477

Reference yield:

: 1365565-61-2
3-(6-(2-((tert-butoxycarbonyl)amino)ethyl)benzo[d][1,3]dioxol-5-yl)propyl methanesulfonate

: 1365565-34-9
(9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 20 °C

4.1: benzene / 32 h / 80 °C / Inert atmosphere

5.1: hydrogenchloride; water / methanol

With hydrogenchloride; water; sodium hydride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1021/jo2025477

Reference yield:

: 1365565-65-6
tert-butyl (2-(6-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)benzo[d][1,3]dioxol-5-yl)ethyl)carbamate

: 1365565-34-9
(9H-fluoren-9-yl)methyl 2-(3-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)propyl)-4,5-dihydroxyphenethylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / 1,4-dioxane

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 20 °C

3: benzene / 32 h / 80 °C / Inert atmosphere

4: hydrogenchloride; water / methanol

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; dichloromethane; benzene;
DOI:10.1021/jo2025477