Technology Process of C58H86N6O10S2
There total 5 articles about C58H86N6O10S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
at 80 ℃;
for 26h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) sodium hydride / 1.) THF, RT
2: 1.) lithium aluminium hydride, sulphuric acid / 1.) THF, 2.) THF
3: 45 percent / Et3N / CH2Cl2 / reflux, RT, 24 h
4: 94 percent / borane THF complex / tetrahydrofuran / 2 h / Heating
5: 27 percent / potassium carbonate / acetonitrile / 26 h / 80 °C
With
lithium aluminium tetrahydride; borane-THF; sulfuric acid; sodium hydride; potassium carbonate; triethylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 45 percent / Et3N / CH2Cl2 / reflux, RT, 24 h
2: 94 percent / borane THF complex / tetrahydrofuran / 2 h / Heating
3: 27 percent / potassium carbonate / acetonitrile / 26 h / 80 °C
With
borane-THF; potassium carbonate; triethylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;