4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl

Base Information

Chemical Name:4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl
CAS No.:1452822-47-7
Molecular Formula:C₃₂H₃₈F₄O₃S
Molecular Weight:578.712
Hs Code.:

Synonyms:

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Chemical Property of 4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl

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Technology Process of 4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl

There total 9 articles about 4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1446303-23-6
1-bromo-4-{2,2,3,3-tetrafluoro-3-[(4-methylphenyl)sulfonyl]propyl}benzene

: 147222-99-9
4-decyloxyphenylboronic acid

: 1452822-47-7
4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; chemoselective reaction; Reflux; Inert atmosphere;
DOI:10.1002/chem.201203315

Reference yield:

: 842141-92-8
1-bromo-4-(3-bromo-2,2,3,3-tetrafluoropropyl)benzene

: 1452822-47-7
4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: sodium dithionite; 3-Methylpyridine / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

2: acetic acid; dihydrogen peroxide / water / 3 h / Reflux

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium dithionite; 3-Methylpyridine; dihydrogen peroxide; potassium carbonate; acetic acid; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; 3: |Suzuki Coupling;
DOI:10.1002/chem.201203315

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1452822-47-7
4-decyloxy-4'-(2,2,3,3-tetrafluoro-3-tosylpropyl)biphenyl

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine hydrate / ethanol

2: copper(l) chloride

3: sodium dithionite; 3-Methylpyridine / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

4: acetic acid; dihydrogen peroxide / water / 3 h / Reflux

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium dithionite; 3-Methylpyridine; dihydrogen peroxide; potassium carbonate; hydrazine hydrate; acetic acid; copper(l) chloride; In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; 5: |Suzuki Coupling;
DOI:10.1002/chem.201203315