Technology Process of Tris[4-(1,1-dimethylethyl)-2-(1H-pyrazol-1-yl)pyridine]cobalt salt with 1,1,1-trifluoro-N-[(trifluoromethyl)sulfonyl]methanesulfonamide (1:3)
There total 1 articles about Tris[4-(1,1-dimethylethyl)-2-(1H-pyrazol-1-yl)pyridine]cobalt salt with 1,1,1-trifluoro-N-[(trifluoromethyl)sulfonyl]methanesulfonamide (1:3) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
cobalt(II) chloride hexahydrate; 2-(1H-pyrazol-1-yl)-4-tert-butylpyridine;
In
methanol; water;
at 70 ℃;
for 0.166667h;
With
hydrogenchloride; dihydrogen peroxide;
In
methanol; water;
at 70 ℃;
for 2h;
bis(trifluoromethane)sulfonimide lithium;
at 50 ℃;
DOI:10.1021/cm400796u