(+)-aphidicolin-15-ene

Base Information

Chemical Name:(+)-aphidicolin-15-ene
CAS No.:41703-78-0
Molecular Formula:C₂₀H₃₂
Molecular Weight:272.474
Hs Code.:

Synonyms:

Suppliers and Price of (+)-aphidicolin-15-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-aphidicolin-15-ene

Chemical Property:

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Technology Process of (+)-aphidicolin-15-ene

There total 7 articles about (+)-aphidicolin-15-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 85706-63-4,93602-51-8
C₂₇H₄₀O₃S

: 41703-78-0,52645-90-6,96193-15-6
(+)-aphidicolin-15-ene

Guidance literature:: With methyl sulfinyl carbanion; In dimethyl sulfoxide; at 60 ℃; for 2h;
DOI:10.1139/v84-331

Reference yield:

: 93519-47-2
C₂₂H₃₆O₂S₂

: 41703-78-0,52645-90-6,96193-15-6
(+)-aphidicolin-15-ene

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / pyridine / 4 h / -5 °C

2: tri-n-butyltin hydride / toluene / 33 h / Heating

3: 75 percent / 1 M KOH in EtOH / 1 h / Heating

4: 86 mg / pyridine / 72 h / 3 °C

5: 60 percent / methyl sulfinyl carbanion / dimethylsulfoxide / 2 h / 60 °C

With pyridine; potassium hydroxide; methyl sulfinyl carbanion; tri-n-butyl-tin hydride; In dimethyl sulfoxide; toluene;
DOI:10.1139/v84-331

Reference yield:

: 93519-49-4,138922-85-7
C₂₇H₃₈O₂

: 41703-78-0,52645-90-6,96193-15-6
(+)-aphidicolin-15-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 1 M KOH in EtOH / 1 h / Heating

2: 86 mg / pyridine / 72 h / 3 °C

3: 60 percent / methyl sulfinyl carbanion / dimethylsulfoxide / 2 h / 60 °C

With pyridine; potassium hydroxide; methyl sulfinyl carbanion; In dimethyl sulfoxide;
DOI:10.1139/v84-331