2-(5-(4-methoxyphenyl)pentylidene)adamantane

Base Information

Chemical Name:2-(5-(4-methoxyphenyl)pentylidene)adamantane
CAS No.:1601475-51-7
Molecular Formula:C₂₂H₃₀O
Molecular Weight:310.48
Hs Code.:

Synonyms:

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Chemical Property of 2-(5-(4-methoxyphenyl)pentylidene)adamantane

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Technology Process of 2-(5-(4-methoxyphenyl)pentylidene)adamantane

There total 13 articles about 2-(5-(4-methoxyphenyl)pentylidene)adamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1601475-45-9
tert-butyl 6-(4-methoxyphenyl)hexanoate

: 1601475-51-7
2-(5-(4-methoxyphenyl)pentylidene)adamantane

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.67 h / -78 °C

1.2: 2 h / -78 - 0 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: triethylamine; 4-Nitrobenzenesulfonyl chloride / dichloromethane / 0 - 20 °C

4.1: 120 °C / Ionic liquid

With triethylamine; trifluoroacetic acid; 4-Nitrobenzenesulfonyl chloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo500577c

Reference yield:

: 107228-87-5
6-(4-methoxyphenyl)-hexan-1-oic acid

: 1601475-51-7
2-(5-(4-methoxyphenyl)pentylidene)adamantane

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: triethylamine / dichloromethane / 2 h / 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.67 h / -78 °C

3.2: 2 h / -78 - 0 °C

4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5.1: triethylamine; 4-Nitrobenzenesulfonyl chloride / dichloromethane / 0 - 20 °C

6.1: 120 °C / Ionic liquid

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; 4-Nitrobenzenesulfonyl chloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo500577c

Reference yield:

: 6-(4-Methoxy-phenyl)-hexanoyl chloride

: 1601475-51-7
2-(5-(4-methoxyphenyl)pentylidene)adamantane

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 2 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.67 h / -78 °C

2.2: 2 h / -78 - 0 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: triethylamine; 4-Nitrobenzenesulfonyl chloride / dichloromethane / 0 - 20 °C

5.1: 120 °C / Ionic liquid

With triethylamine; trifluoroacetic acid; 4-Nitrobenzenesulfonyl chloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo500577c