3-N-amino- butanoic acid methyl ester

Base Information

• Chemical Name: 3-N-amino- butanoic acid methyl ester
• CAS No.: 137132-14-0
• Molecular Formula: C₁₆H₂₅N₂O₆P
• Molecular Weight: 372.358

Synonyms:

Chemical Property of 3-N-amino- butanoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 3-N-amino- butanoic acid methyl ester

There total 2 articles about 3-N-amino- butanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyloxycarbonyl-1-aminoethanephosphonic acid methyl monoester (61989-17-1) → 3-N-amino- butanoic acid methyl ester (137132-14-0)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃ / 4 h / Ambient temperature

2: Et₃N / CHCl₃ / 1 h / Ambient temperature

With thionyl chloride; triethylamine; In chloroform;

DOI:10.1016/0223-5234(91)90057-T

Reference yield:

C11H15ClNO4P (107072-65-1) + (3RS)-3-aminobutanoic acid methyl ester hydrochloride (137132-12-8) → 3-N-amino- butanoic acid methyl ester (137132-14-0)

Guidance literature:

With triethylamine; In chloroform; for 1h; Yield given; Ambient temperature;

DOI:10.1016/0223-5234(91)90057-T

Reference yield:

3-N-amino- butanoic acid methyl ester (137132-14-0) → 3-N-amino- butanoic acid, disodium salt (137132-08-2,137132-16-2)

Guidance literature:

With sodium hydroxide; for 24h; Ambient temperature;

DOI:10.1016/0223-5234(91)90057-T

upstream raw materials:

C₁₁H₁₅ClNO₄P

(3RS)-3-aminobutanoic acid methyl ester hydrochloride

N-benzyloxycarbonyl-1-aminoethanephosphonic acid methyl monoester

Downstream raw materials:

3-N-amino- butanoic acid, disodium salt

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