C₂₄H₂₁F₃N₄O₃

Base Information

Chemical Name:C₂₄H₂₁F₃N₄O₃
CAS No.:1431701-27-7
Molecular Formula:C₂₄H₂₁F₃N₄O₃
Molecular Weight:470.451
Hs Code.:

C<sub>24</sub>H<sub>21</sub>F<sub>3</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₄H₂₁F₃N₄O₃

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Technology Process of C₂₄H₂₁F₃N₄O₃

There total 5 articles about C₂₄H₂₁F₃N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 359-41-1
1,1,1-trifluoro-2,3-epoxypropane

: 1431702-85-0
C₂₁H₁₈N₄O₂

: 1431701-27-7,1431701-28-8,1431701-29-9
C₂₄H₂₁F₃N₄O₃

Guidance literature:: C₂₁H₁₈N₄O₂; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 5 ℃; for 1h; Inert atmosphere;

1,1,1-trifluoro-2,3-epoxypropane; In N,N-dimethyl-formamide; mineral oil; at 70 ℃; for 4h;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1431701-27-7,1431701-28-8,1431701-29-9
C₂₄H₂₁F₃N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 80 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

4.2: 4 h / 70 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; sodium hydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1431701-27-7,1431701-28-8,1431701-29-9
C₂₄H₂₁F₃N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 80 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

4.2: 4 h / 70 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; sodium hydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;