[(PhNH)P₂(NPh)2]2NPh

Base Information

• Chemical Name: [(PhNH)P₂(NPh)2]2NPh
• CAS No.: 73181-31-4
• Molecular Formula: C₄₂H₃₇N₇P₄
• Molecular Weight: 763.698

Synonyms:

Chemical Property of [(PhNH)P₂(NPh)2]2NPh

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of [(PhNH)P₂(NPh)2]2NPh

There total 2 articles about [(PhNH)P₂(NPh)2]2NPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

aniline (62-53-3) → [(PhNH)P2(NPh)2]2NPh (73181-31-4,99603-12-0)

Guidance literature:

With phosphorus trichloride; In toluene; at 110 ℃;

DOI:10.1016/j.tet.2010.01.099

Reference yield:

→ [(PhNH)P2(NPh)2]2NPh (73181-31-4,99603-12-0)

Guidance literature:

PCl3, PhNH2 (als CH2Cl2-Addukt isoliert);

DOI:10.1039/C39790000647

Reference yield: 74.0%

(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0) (12146-37-1,124717-04-0) + [(PhNH)P2(NPh)2]2NPh (73181-31-4,99603-12-0) → Mo(CO)4(((C6H5NH)P2(NC6H5)2)2NC6H5)*C7H8 (104130-73-6)

Guidance literature:

In toluene; N2 atmosphere, 25°C, 5 h; filtration, reduced volume, crystn. (0°C); elem. anal.;

upstream raw materials:

aniline

Downstream raw materials:

Mo(CO)4(((C₆H₅NH)P₂(NC₆H₅)2)2NC₆H₅)*C₇H₈

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