C₂₆H₂₇ClN₂O₄

Base Information

Chemical Name:C₂₆H₂₇ClN₂O₄
CAS No.:1256250-98-2
Molecular Formula:C₂₆H₂₇ClN₂O₄
Molecular Weight:466.964
Hs Code.:

C<sub>26</sub>H<sub>27</sub>ClN<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₆H₂₇ClN₂O₄

Chemical Property:

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Technology Process of C₂₆H₂₇ClN₂O₄

There total 5 articles about C₂₆H₂₇ClN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256254-43-9
C₁₄H₁₉Cl₂NO₃

: 1256250-98-2
C₂₆H₂₇ClN₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: palladium diacetate; 1,3-bis(dicyclohexylphosphino)propane bis(tetrafluoroborate) salt; potassium carbonate / N,N-dimethyl-formamide

2: potassium carbonate; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / N,N-dimethyl-formamide; water

3: lithium hydroxide; water / tetrahydrofuran

4: water; diphenyl phosphoryl azide / toluene / Heating

5: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; 1,3-bis(dicyclohexylphosphino)propane bis(tetrafluoroborate) salt; diphenyl phosphoryl azide; water; palladium diacetate; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; 2: |Suzuki Coupling / 4: |Curtius Rearrangement;
DOI:10.1021/acsmedchemlett.6b00194

Reference yield:

: C₁₆H₂₂ClNO₅

: 1256250-98-2
C₂₆H₂₇ClN₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / N,N-dimethyl-formamide; water

2: lithium hydroxide; water / tetrahydrofuran

3: water; diphenyl phosphoryl azide / toluene / Heating

4: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; diphenyl phosphoryl azide; water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; 1: |Suzuki Coupling / 3: |Curtius Rearrangement;
DOI:10.1021/acsmedchemlett.6b00194

Reference yield:

: C₂₂H₂₆ClNO₅

: 1256250-98-2
C₂₆H₂₇ClN₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide; water / tetrahydrofuran

2: water; diphenyl phosphoryl azide / toluene / Heating

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With diphenyl phosphoryl azide; water; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 2: |Curtius Rearrangement;
DOI:10.1021/acsmedchemlett.6b00194