2-(phenylthio)dimethylphosphinoethane

Base Information

Chemical Name:2-(phenylthio)dimethylphosphinoethane
CAS No.:250709-79-6
Molecular Formula:C₁₀H₁₅PS
Molecular Weight:198.269
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(phenylthio)dimethylphosphinoethane

Chemical Property:

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Technology Process of 2-(phenylthio)dimethylphosphinoethane

There total 1 articles about 2-(phenylthio)dimethylphosphinoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

tetramethyldiphosphane: 3676-91-3
tetramethyldiphosphane

: 5535-49-9
2-Chloroethyl phenyl sulfide

: 250709-79-6
2-(phenylthio)dimethylphosphinoethane

Guidance literature:: With sodium; In ammonia; for 2h;
DOI:10.1016/S0022-328X(99)00334-4

Reference yield: 71.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 143-66-8
sodium tetraphenyl borate

: 250709-79-6
2-(phenylthio)dimethylphosphinoethane

: 250709-71-8
[RuCl(cymene)(2-(phenylthio)dimethylphosphinoethane)][B(C₆H₅)4]

Guidance literature:: In ethanol; N2-atmosphere; stirring Ru-complex with ligand at room temp. overnight, evapn. (reduced pressure), extn. into EtOH, addn. of NaBPh4 (pptn.); recrystn. (CH2Cl2/Et2O); elem. anal.;
DOI:10.1016/S0022-328X(99)00334-4

Reference yield: 7.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 250709-79-6
2-(phenylthio)dimethylphosphinoethane

: 251105-28-9
trans(Cl,Cl')cis(P,P')-[RuCl₂(2-(phenylthio)dimethylphosphinoethane)2]

: 251105-28-9
trans(Cl,Cl')trans(P,P')-[RuCl₂(2-(phenylthio)dimethylphosphinoethane)2]

: cis(Cl,Cl')cis(P,P')-[RuCl₂(2-(phenylthio)dimethylphosphinoethane)2]

Guidance literature:: In butan-1-ol; N2-atmosphere; refluxing Ru-complex with excess of P,S-ligand overnight (pptn.); filtration, evapn., extn. into Et2O, evapn., washing (hexane), recrystn.(PhMe); elem. anal.; other isomers by fractional extn. of initial ppt.;
DOI:10.1016/S0022-328X(99)00334-4