C₂₂H₃₆O₅Si

Base Information

Chemical Name:C₂₂H₃₆O₅Si
CAS No.:1279710-34-7
Molecular Formula:C₂₂H₃₆O₅Si
Molecular Weight:408.61
Hs Code.:

C<sub>22</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₂₂H₃₆O₅Si

Chemical Property:

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Technology Process of C₂₂H₃₆O₅Si

There total 10 articles about C₂₂H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279710-32-5
C₂₂H₃₈O₅Si

: 1279710-34-7
C₂₂H₃₆O₅Si

Guidance literature:: C₂₂H₃₈O₅Si; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃;

With triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2011.01.042

Reference yield:

: 1279710-25-6
C₂₈H₅₀O₄Si₂

: 1279710-34-7
C₂₂H₃₆O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / -35 - -25 °C

2: hydrogen / benzene / 24 °C

3: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / -25 °C / Molecular sieve

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 °C

5: camphor-10-sulfonic acid / dichloromethane / 0 °C

6: pyridine / 0 °C

7: 2,6-dimethylpyridine / dichloromethane / 0 °C

8: diisobutylaluminium hydride / dichloromethane / -78 °C

9: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; oxalyl dichloride; diethyl (2S,3S)-tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; benzene; 3: Katsuki-Sharpless epoxidation / 9: Swern oxidation / 9: Swern oxidation;
DOI:10.1016/j.tetlet.2011.01.042

Reference yield:

: 1279710-26-7
C₂₂H₃₆O₄Si

: 1279710-34-7
C₂₂H₃₆O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogen / benzene / 24 °C

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / -25 °C / Molecular sieve

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 °C

4: camphor-10-sulfonic acid / dichloromethane / 0 °C

5: pyridine / 0 °C

6: 2,6-dimethylpyridine / dichloromethane / 0 °C

7: diisobutylaluminium hydride / dichloromethane / -78 °C

8: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; oxalyl dichloride; diethyl (2S,3S)-tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; benzene; 2: Katsuki-Sharpless epoxidation / 8: Swern oxidation / 8: Swern oxidation;
DOI:10.1016/j.tetlet.2011.01.042