Technology Process of 3,5-dichloro-2,2',6,6'-tetramethoxy-4'-methylbenzophenone
There total 5 articles about 3,5-dichloro-2,2',6,6'-tetramethoxy-4'-methylbenzophenone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 61 percent / sulfuryl chloride / diethyl ether / 2 h / Ambient temperature
2: 90 percent / K2CO3 / acetone / 16 h / Ambient temperature
3: 78 percent / KOH / H2O; dimethylsulfoxide / 24 h / 80 - 90 °C
4: SOCl2 / toluene / 2 h / Heating
5: 1.) BuLi / 1.) ether, hexane, RT, 3 h, 2.) RT, 2 h
With
potassium hydroxide; n-butyllithium; thionyl chloride; sulfuryl dichloride; potassium carbonate;
In
diethyl ether; water; dimethyl sulfoxide; acetone; toluene;
DOI:10.1071/CH9901773
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 78 percent / KOH / H2O; dimethylsulfoxide / 24 h / 80 - 90 °C
2: SOCl2 / toluene / 2 h / Heating
3: 1.) BuLi / 1.) ether, hexane, RT, 3 h, 2.) RT, 2 h
With
potassium hydroxide; n-butyllithium; thionyl chloride;
In
water; dimethyl sulfoxide; toluene;
DOI:10.1071/CH9901773
- Guidance literature:
-
Multi-step reaction with 2 steps
1: SOCl2 / toluene / 2 h / Heating
2: 1.) BuLi / 1.) ether, hexane, RT, 3 h, 2.) RT, 2 h
With
n-butyllithium; thionyl chloride;
In
toluene;
DOI:10.1071/CH9901773
