3,4-cis-3,2'-threo-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

Base Information

Chemical Name:3,4-cis-3,2'-threo-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane
CAS No.:121664-63-9
Molecular Formula:C₁₅H₁₉BrN₂O₂S₂
Molecular Weight:403.364
Hs Code.:

3,4-cis-3,2'-threo-4-<O-<N-(p-bromophenyl)carbamoyl>>oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

Synonyms:

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Chemical Property of 3,4-cis-3,2'-threo-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

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Technology Process of 3,4-cis-3,2'-threo-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

There total 10 articles about 3,4-cis-3,2'-threo-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 103781-95-9,121702-91-8,121702-92-9,121702-93-0,131488-77-2,131488-78-3,131488-82-9
3,4-trans-3,2'-erythro-4-Hydroxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

: 2493-02-9
4-bromophenyl isocyanate

: 121664-63-9,121702-94-1,121702-95-2,125356-07-2,125409-37-2
3,4-trans-3,2'-erythro-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

Guidance literature:: With triethylamine; In toluene; at 60 ℃;

Reference yield: 51.0%

: 103781-95-9,121702-91-8,121702-92-9,121702-93-0,131488-77-2,131488-78-3,131488-82-9
3,4-cis-3,2'-threo-4-Hydroxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

: 2493-02-9
4-bromophenyl isocyanate

: 121664-63-9,121702-94-1,121702-95-2,125356-07-2,125409-37-2
3,4-cis-3,2'-threo-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

Guidance literature:: With triethylamine; In toluene; at 60 ℃; for 0.5h;

Reference yield:

: 826-41-5
N-Methyl-2,2-diethoxypyrrolidine

: 121664-63-9,121702-94-1,121702-95-2,125356-07-2,125409-37-2
3,4-trans-3,2'-erythro-4->oxy-3-(1-methylpyrrolidin-2-yl)-1,2-dithiolane

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / toluene / 100 °C

2: 56 percent / NaBH₄, glacial acetic acid / Ambient temperature

3: Na, ammonia

4: 10 percent aq. ferric chloride, air

5: 53 percent / triethylamine / toluene / 60 °C

With sodium tetrahydroborate; air; ammonia; sodium; iron(III) chloride; acetic acid; triethylamine; In toluene;