Technology Process of C26H32ClN3O3
There total 9 articles about C26H32ClN3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: trifluoroacetic acid / toluene / 0 - 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C
3: triethylamine / tetrahydrofuran / 0 °C
4: dimethyl sulfoxide / 90 °C
5: water; sodium hydroxide / methanol / Reflux
6: dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C
7: Wilkinson's catalyst / water; acetonitrile / Reflux
8: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
With
Wilkinson's catalyst; lithium aluminium tetrahydride; water; sodium tris(acetoxy)borohydride; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2011.02.046
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethyl sulfoxide / 90 °C
2: water; sodium hydroxide / methanol / Reflux
3: dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C
4: Wilkinson's catalyst / water; acetonitrile / Reflux
5: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
With
Wilkinson's catalyst; water; sodium tris(acetoxy)borohydride; dicyclohexyl-carbodiimide; sodium hydroxide;
In
methanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.02.046