[Cu(H₂O)(2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O

Base Information

• Chemical Name: [Cu(H₂O)(2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O
• CAS No.: 918794-51-1
• Molecular Formula: C₂₀H₁₅CuN₃O₄*H₂O
• Molecular Weight: 442.918

Synonyms:

Chemical Property of [Cu(H₂O)(2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [Cu(H₂O)(2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O

There total 1 articles about [Cu(H₂O)(2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

copper diacetate trihydrate + 2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid (918794-63-5) → [Cu(H2O)(2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H2O (918794-51-1)

Guidance literature:

With sodium hydroxide; In ethanol; water; addn. of soln. of Cu(CH3COO)2*3H2O in EtOH-H2O (1:1) to hot soln. of 2-(5-phenyl azo-2-hydroxy benzylidene amino) benzoic acid in 95% EtOH; adjusting pH to 6-7 with alcoholic NaOH (0.01 M); stirring at 70°C for 30 min; concn. by evapn. for 1 d; filtration, washing with EtOH and Et2O, dryingunder vac., recrystn. from EtOH-water (1:1); elem. anal.;

DOI:10.1016/j.saa.2006.01.049

upstream raw materials:

2-[5-phenyl azo-2-hydroxy benzylidene amino]benzoic acid

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