2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine

Base Information

Chemical Name:2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine
CAS No.:131769-80-7
Molecular Formula:C₂₉H₂₅N₅O₅
Molecular Weight:523.548
Hs Code.:

2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzo<c>phenanthridine

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Chemical Property of 2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine

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Technology Process of 2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine

There total 8 articles about 2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 14210-25-4
5-Chloro-1-phenyltetrazole

: 2-ethoxy-3,8,9-trimethoxybenzophenanthridin-12-ol sulfate

: 131769-80-7
2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine

Guidance literature:: With sodium carbonate; In acetone; Heating;

Reference yield:

: 131769-73-8
4-Ethoxycarbonylmethyl-3-(4-ethoxy-3-methoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-4-ol

: 131769-80-7
2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / concd. sulfuric acid / 0.5 h

2: 77 percent / anhydr. sodium carbonate / acetone / Heating

With sulfuric acid; sodium carbonate; In acetone;

Reference yield:

: 131769-66-9
2-(4-Ethoxy-3-methoxyphenyl)-2-(3,4-dimethoxybenzylamino)acetonitrile

: 131769-80-7
2-Ethoxy-3,8,9-trimethoxy-12-(1-phenyl-1H-tetrazol-5-yloxy)benzophenanthridine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / anhydr. hydrogen fluoride / 24 h

2: 65 percent / zinc, trimethylsilyl chloride / dioxane; various solvent(s) / 24 h / Ambient temperature

3: 66 percent / concd. sulfuric acid / 0.5 h

4: 77 percent / anhydr. sodium carbonate / acetone / Heating

With chloro-trimethyl-silane; sulfuric acid; hydrogen fluoride; sodium carbonate; zinc; In 1,4-dioxane; acetone;