[PdBr(C₆H₃(CH₂SPh)2-2,6)]

Base Information

Chemical Name:[PdBr(C₆H₃(CH₂SPh)2-2,6)]
CAS No.:1160761-78-3
Molecular Formula:C₂₀H₁₇BrPdS₂
Molecular Weight:507.811
Hs Code.:

[PdBr(C<sub>6</sub>H<sub>3</sub>(CH<sub>2</sub>SPh)2-2,6)]

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Chemical Property of [PdBr(C₆H₃(CH₂SPh)2-2,6)]

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Technology Process of [PdBr(C₆H₃(CH₂SPh)2-2,6)]

There total 1 articles about [PdBr(C₆H₃(CH₂SPh)2-2,6)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 52522-40-4
tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex

: 201865-04-5
C₆H₃(CH₂SPh)2-2,6-Br-1

: 1160761-78-3,1065473-22-4,1064656-24-1
[PdBr(C₆H₃(CH₂SPh)2-2,6)]

Guidance literature:: In benzene; (N2); using Schlenk techniques; addn. of Pd2(dba)3*CHCl3 to soln. of C6H3(CH2SPh)2-2,6-Br-1 in benzene; stirring at room temp. for 16 h; removal of solvent under reduced pressure, dissolving in CH2Cl2, filtration, concn., addn. of Et2O, pptn., second pptn. from CH2Cl2; drying in vac., elem. anal.;
DOI:10.1021/om800324w

Reference yield: 27.0%

: 1160761-78-3,1065473-22-4,1064656-24-1
[PdBr(C₆H₃(CH₂SPh)2-2,6)]

: 7732-18-5
water

: silver sulfate

: 2Pd⁽²⁺⁾*2C₆H₃(CH₂SC₆H₅)2^(1-)*SO₄^(2-)*2H₂O=C₄₀H₃₄O₄Pd₂S₅*2H₂O

Guidance literature:: In water; byproducts: AgBr; Pd-complex suspended in soln. of Ag2SO4 in H2O, stirred for 1 wk in darkin air; filtered, washed with H2O, concd. in vacuo, ppt. dissolved in acetone, filtered; elem. anal.;
DOI:10.1039/b816936e