(S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid

Base Information

Chemical Name:(S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid
CAS No.:143747-59-5
Molecular Formula:C₂₁H₂₃Cl₂NO₃
Molecular Weight:408.325
Hs Code.:

(S)-(+)-1-<2-<bis(4-chlorophenyl)methoxy>ethyl>-3-piperidinecarboxylic acid

Synonyms:

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Chemical Property of (S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid

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Technology Process of (S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid

There total 5 articles about (S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-97-1
4,4'-dichlorobenzophenone

: 143747-59-5
(S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: conc. H₂SO₄ / toluene / 2 h / 85 - 90 °C

2: K₂CO₃ / acetonitrile / 15 h / Heating

3: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

With lithium hydroxide; sulfuric acid; potassium carbonate; In methanol; toluene; acetonitrile;
DOI:10.1021/jm00100a032

Reference yield:

: 221916-05-8
1-bromo-2-[bis(4-chlorophenyl)methoxy]ethane

: 143747-59-5
(S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetonitrile / 15 h / Heating

2: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

With lithium hydroxide; potassium carbonate; In methanol; acetonitrile;
DOI:10.1021/jm00100a032

Reference yield:

: 110283-43-7
1-<2-ethyl>-3-piperidinecarboxylic acid ethyl ester

: 143747-59-5
(S)-(+)-1-<2-ethyl>-3-piperidinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

With lithium hydroxide; In methanol;
DOI:10.1021/jm00100a032