C₂₂H₃₀O₂Si

Base Information

Chemical Name:C₂₂H₃₀O₂Si
CAS No.:1173695-83-4
Molecular Formula:C₂₂H₃₀O₂Si
Molecular Weight:354.565
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>2</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₀O₂Si

Chemical Property:

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Technology Process of C₂₂H₃₀O₂Si

There total 1 articles about C₂₂H₃₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1173695-82-3
C₂₃H₃₀O₃Si

: 1173695-83-4
C₂₂H₃₀O₂Si

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 1h;
DOI:10.1016/j.tetlet.2009.04.039

Reference yield:

: 1173695-83-4
C₂₂H₃₀O₂Si

: 1173695-68-5
C₂₂H₂₈O₂Si

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 10h;
DOI:10.1016/j.tetlet.2009.04.039

Reference yield:

: 1173695-83-4
C₂₂H₃₀O₂Si

: 17015-63-3,100428-91-9,10309-44-1
(S,E)-1-(3,7-dimethyl-3-vinylocta-1,6-dien-1-yl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 9 steps

1.1: Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: C₄₆H₅₁O₅P; chloro(1,5-cyclooctadiene)rhodium(I) dimer; silver tetrafluoroborate; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

4.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

4.2: 2 h / -78 °C / Inert atmosphere

4.3: 2 h / -78 - 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride; water / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex; dimethyl sulfoxide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 - 20 °C / Inert atmosphere

7.2: 24 h / -78 - 20 °C / Inert atmosphere

8.1: Lawessons reagent / toluene / 6 h / Inert atmosphere; Reflux

9.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

9.2: 9 h / -78 - 20 °C / Inert atmosphere

With Lawessons reagent; silver tetrafluoroborate; chloro(1,5-cyclooctadiene)rhodium(I) dimer; n-butyllithium; C₄₆H₅₁O₅P; tetrabutyl ammonium fluoride; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; toluene; 6.1: |Parikh-Doering Oxidation / 7.1: |Wittig Olefination / 7.2: |Wittig Olefination;
DOI:10.1021/jacs.7b02324