o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide

Base Information

• Chemical Name: o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide
• CAS No.: 82057-59-8
• Molecular Formula: C₅₂H₇₇N₁₃O₁₄S₂
• Molecular Weight: 1172.39

Synonyms:

Chemical Property of o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide

There total 4 articles about o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(S)-3-(4-Dimethylamino-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionic acid 2,4,5-trichloro-phenyl ester (84796-40-7) + 3-((S)-3-{(S)-2-[(S)-2-((2S,3S)-2-Amino-3-methyl-pentanoylamino)-4-carbamoyl-butyrylamino]-3-carbamoyl-propionylamino}-4-{(S)-2-[(S)-1-(carbamoylmethyl-carbamoyl)-3-methyl-butylcarbamoyl]-pyrrolidin-1-yl}-4-oxo-butylsulfanyl)-propionic acid (30905-50-1) → o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide (82057-59-8)

Guidance literature:

In N,N-dimethyl-formamide;

Reference yield:

p-Dimethylamino-L-phenylalanin (84796-32-7,1991-95-3) → o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide (82057-59-8)

Guidance literature:

Multi-step reaction with 3 steps

2: 84 percent

3: 96 percent / dimethylformamide

In N,N-dimethyl-formamide;

Reference yield:

(S)-3-(4-Dimethylamino-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionic acid (82057-64-5) → o-nitrobenzenesulfenyl-p-dimethylaminophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(β-carboxyethyl)homocysteinyl-prolyl-leucyl-glycine amide (82057-59-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent

2: 96 percent / dimethylformamide

In N,N-dimethyl-formamide;

upstream raw materials:

(S)-3-(4-Dimethylamino-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionic acid 2,4,5-trichloro-phenyl ester

3-((S)-3-{(S)-2-[(S)-2-((2S,3S)-2-Amino-3-methyl-pentanoylamino)-4-carbamoyl-butyrylamino]-3-carbamoyl-propionylamino}-4-{(S)-2-[(S)-1-(carbamoylmethyl-carbamoyl)-3-methyl-butylcarbamoyl]-pyrrolidin-1-yl}-4-oxo-butylsulfanyl)-propionic acid

p-Dimethylamino-L-phenylalanin

(S)-3-(4-Dimethylamino-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionic acid

Downstream raw materials:

<2-p-dimethylaminophenylalanine>deamino-6-carba-oxytocin

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