(3S)-3-hydroxy-vinyl-β-ionol

Base Information

Chemical Name:(3S)-3-hydroxy-vinyl-β-ionol
CAS No.:1200124-92-0
Molecular Formula:C₁₅H₂₄O₂
Molecular Weight:236.354
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-3-hydroxy-vinyl-β-ionol

Chemical Property:

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Technology Process of (3S)-3-hydroxy-vinyl-β-ionol

There total 2 articles about (3S)-3-hydroxy-vinyl-β-ionol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38963-41-6
(rac)-4-(4-hydroxy-2,6,6-trimethyl-2-cyclohexen-1-yl)-3-buten-2-one

: 1200124-92-0
(3S)-3-hydroxy-vinyl-β-ionol

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / tetrahydrofuran; methanol / 1 h / 50 °C / Inert atmosphere

2: immobilized lipase Pseudomonas cepacia / ethyl acetate / 20 h / 20 °C / Inert atmosphere; Enzymatic reaction

3: tetrahydrofuran; toluene / 1.5 h / -20 °C / Inert atmosphere

With potassium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; toluene;
DOI:10.1055/s-0030-1258382

Reference yield:

: 116296-75-4
(rac)-(E)-4-(4-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-2-one

: 1200124-92-0
(3S)-3-hydroxy-vinyl-β-ionol

Guidance literature:: Multi-step reaction with 2 steps

1: immobilized lipase Pseudomonas cepacia / ethyl acetate / 20 h / 20 °C / Inert atmosphere; Enzymatic reaction

2: tetrahydrofuran; toluene / 1.5 h / -20 °C / Inert atmosphere

With immobilized lipase Pseudomonas cepacia; In tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1055/s-0030-1258382

Reference yield:

: 1200124-92-0
(3S)-3-hydroxy-vinyl-β-ionol

: 1200446-88-3
all-E-(3S)-β-cryptoxanthin

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; water / 0 - 20 °C

2: ethyloxirane / ethanol / 6 h / Inert atmosphere; Reflux

With ethyloxirane; In methanol; ethanol; water; 1: Wittig reaction;
DOI:10.1055/s-0030-1258382