C₁₇H₁₃⁽²⁾HN₂O

Base Information

Chemical Name:C₁₇H₁₃⁽²⁾HN₂O
CAS No.:1276540-20-5
Molecular Formula:C₁₇H₁₄N₂O
Molecular Weight:263.303
Hs Code.:

C<sub>17</sub>H<sub>13</sub><sup>(2)</sup>HN<sub>2</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₃⁽²⁾HN₂O

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Technology Process of C₁₇H₁₃⁽²⁾HN₂O

There total 2 articles about C₁₇H₁₃⁽²⁾HN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1276539-84-4
2-((3-phenylprop-2-ynyloxy)methyl)-1H-benzo[d]imidazole

: C₁₇H₁₃⁽²⁾HN₂O

: 1276540-20-5
C₁₇H₁₃⁽²⁾HN₂O

Guidance literature:: With water-d2; silver trifluoromethanesulfonate; at 150 ℃; for 0.25h; regioselective reaction; Inert atmosphere; Sealed vial; Microwave irradiation;
DOI:10.1039/c0gc00668h

Reference yield:

: 1226870-14-9
C₈H₁₂O₃

: C₁₇H₁₃⁽²⁾HN₂O

: 1276540-20-5
C₁₇H₁₃⁽²⁾HN₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine / 0.08 h / 20 °C

1.2: 2 h / 20 °C

2.1: water; sodium hydroxide / tetrahydrofuran / 3 h / 20 °C

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / methanol / 20 °C

4.1: acetic acid / 5 h / 90 °C / Inert atmosphere; neat (no solvent)

5.1: water-d2; silver trifluoromethanesulfonate / 0.25 h / 150 °C / Inert atmosphere; Sealed vial; Microwave irradiation

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; water-d2; silver trifluoromethanesulfonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1039/c0gc00668h