(+/-)-Cortysaeure

Base Information

• Chemical Name: (+/-)-Cortysaeure
• CAS No.: 122674-23-1
• Molecular Formula: C₁₅H₂₂O₂
• Molecular Weight: 234.338
• Mol file: 122674-23-1.mol

Synonyms:

Chemical Property of (+/-)-Cortysaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-Cortysaeure

There total 7 articles about (+/-)-Cortysaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dl-β-costal (3650-40-6,76497-23-9,88564-53-8) → (+/-)-Cortysaeure (3650-43-9,122674-23-1)

Guidance literature:

With sodium hydroxide; silver nitrate;

DOI:10.1021/jo01347a045

Reference yield:

Methanesulfonic acid (2S,4aR,8aS)-4a-methyl-8-methylene-decahydro-naphthalen-2-yl ester (4966-46-5) → (+/-)-Cortysaeure (3650-43-9,122674-23-1)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH

2: (i) NaH, (ii) LiAlH₄, (iii) MnO₂

3: AgNO₃, aq. NaOH

With sodium hydroxide; sodium hydride; silver nitrate;

DOI:10.1021/jo01347a045

Reference yield:

1-Methylen-10-ref-methyl-7-cis-tosyloxy-9H-trans-decalin → (+/-)-Cortysaeure (3650-43-9,122674-23-1)

Guidance literature:

Multi-step reaction with 6 steps

1: H₂O

2: NaOH

3: Py

4: NaH

5: (i) NaH, (ii) LiAlH₄, (iii) MnO₂

6: AgNO₃, aq. NaOH

With pyridine; sodium hydroxide; water; sodium hydride; silver nitrate;

DOI:10.1021/jo01347a045

upstream raw materials:

dl-β-costal

Methanesulfonic acid (2S,4aR,8aS)-4a-methyl-8-methylene-decahydro-naphthalen-2-yl ester