Technology Process of C65H72BrNO14SSi
There total 8 articles about C65H72BrNO14SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / chloroform
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 4 h
3: dmap; triethylamine / dichloromethane
With
pyridine; dmap; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; chloroform; water;
DOI:10.1038/nchem.1073
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 4 h
2: dmap; triethylamine / dichloromethane
With
dmap; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; water;
DOI:10.1038/nchem.1073
- Guidance literature:
-
Multi-step reaction with 9 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h
2: dmap; triethylamine / dichloromethane
3: sodium hydride / N,N-dimethyl-formamide
4: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 4 h / -78 - -20 °C
5: copper(II) bis(trifluoromethanesulfonate)
6: zinc(II) iodide / dichloromethane / 3 h
7: pyridine / chloroform
8: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 4 h
9: dmap; triethylamine / dichloromethane
With
pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; trimethylsilyl trifluoromethanesulfonate; copper(II) bis(trifluoromethanesulfonate); sodium hydride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc(II) iodide;
In
dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1038/nchem.1073
