C₂₂H₂₂F₄N₂O₂

Base Information

Chemical Name:C₂₂H₂₂F₄N₂O₂
CAS No.:1002129-24-9
Molecular Formula:C₂₂H₂₂F₄N₂O₂
Molecular Weight:422.422
Hs Code.:

C<sub>22</sub>H<sub>22</sub>F<sub>4</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₂H₂₂F₄N₂O₂

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Technology Process of C₂₂H₂₂F₄N₂O₂

There total 5 articles about C₂₂H₂₂F₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 1002129-23-8
C₁₈H₁₆F₄N₂O

: 1002129-24-9
C₂₂H₂₂F₄N₂O₂

Guidance literature:: With sodium hydride; In toluene; at 100 ℃; for 120h; Inert atmosphere;
DOI:10.1021/jm300101n

Reference yield:

: 110-89-4
piperidine

: 1002129-24-9
C₂₂H₂₂F₄N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: water / 25 h / 20 °C / Inert atmosphere

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 14 h / 20 °C / Inert atmosphere

3: tetrahydrofuran / 29 h / 20 °C / Inert atmosphere

4: sodium hydride / toluene / 120 h / 100 °C / Inert atmosphere

With sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; 4: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jm300101n

Reference yield:

: 1002129-22-7
C₁₄H₁₈F₃N₃O₂

: 1002129-24-9
C₂₂H₂₂F₄N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 29 h / 20 °C / Inert atmosphere

2: sodium hydride / toluene / 120 h / 100 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; toluene; 2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jm300101n